Spanish judges ordered Catalan lawmakers today to suspend a planned session that could see the region declare independence as the national government rejected calls for mediation in a volatile standoff.
The move raised the stakes in Spain's deepest political crisis in a generation.
Violence erupted last weekend during Catalonia's independence referendum outlawed by Madrid.
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But Prime Minister Mariano Rajoy's office retorted that the government "will not accept blackmail."
Rajoy himself today called on Catalan leaders to "return to legality," in an interview with the Spanish news agency EFE.
Catalan leaders have threatened to declare independence within days -- possibly during Monday's plenary session in the regional parliament.
But the Constitutional Court today ordered the session to be suspended while it hears an appeal by rival politicians.
It warned that any session carried out in defiance of its ban would be "null."
It said the parliament's leaders could face criminal action if they ignore the court order.
Puigdemont and other Catalan leaders have said they are not afraid of going to jail over their independence bid.
They carried out the referendum in defiance of a ban by the Spanish court and stern warnings from the national government in Madrid.
Today's ruling raised the question of how the Spanish state will respond if Catalans decide to push ahead with Monday's session.
The vote on Sunday saw shocking scenes of police with batons beating unarmed voters.
The vote was not carried out according to regular electoral standards but Puigdemont said it had lent legitimacy to the independence drive.
If Catalonia declares independence, Spain could respond by suspending the region's existing autonomous status and imposing direct rule from Madrid.
The speaker of the Catalan parliament Carme Forcadell warned such a move "would just increase support for the pro- independence side."
Catalan authorities claim 42 per cent of voters cast ballots in the referendum and that 90 per cent of those backed independence.
Madrid has branded the vote a "farce" and Spain's King Felipe VI sided with the central government, accusing separatist leaders of endangering Spain's "stability.
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